200L double layer jacketed glass reactor
Product introduction:
This machine has electric constant speed stirring system, condensation and dropping system. The interlayer of kettle body needs to be connected with heating or cooling circulation equipment. When the material is stirred, the circulating hot solution or cooling liquid is injected through the interlayer to make the materials in the kettle are heated or cooled at a constant temperature. When the material is heated and reacted, the evaporation efficiency can be improved under vacuum conditions (
a
vacuum device need to be connected). The solvent vapor is cooled into liquid when passing through the glass condensing coil (
a
cooling device need to be connected)
,
which can be refluxed
i
nto the kettle
.
I
t can also be rec
ycled
through the lower valve of the
dean-stark
.
When
the reaction is completed, the material can be discharged from the side outlet at the bottom of the kettle.
This series of products need to be equipped with a vacuum device, a high-temperature or low-temperature circulation device
to form
system devices.
Basic configuration:
• The parts in contact with the material are all made of high borosilicate glass (expansion coefficient 3.3) and PTFE materials, which have stable performance and are not easy to react with the materials.
• Using aluminum alloy + stainless steel material as
frame
body
• Glass + PTFE discharge valve,
side
material
discharge
without effusion
.
• Low-speed power-increasing motor, electronic stepless speed regulation, fine
adjustment
by
knob
, speed control box
with dual display function
can digitally display the speed and the temperature of the material in the kettle.
•
The
stirr
ing system adopts ceramic bearings and mechanical seals to prevent the stirring rod from wearing out
.
•
Using PT100 temperature sensor, 304 stainless steel material, wrapped
by
transparent PTFE tube
outside
, double anti-corrosion
.
•
Vacuum pressure gauge s
hows
real-time vacuum
by
pointer
.
•
Crescent-type stirring paddle, 304 stainless steel + PTFE stirring blade; the material of the stirring rod is 304 stainless steel, and it is wrapped
in
PTFE tube outside.
• There is a universal wheel with brake at the bottom of the equipment, which can be moved as a whole and
be operated conveniently.
•
F
use safety protection
Technical parameter:
| Model | HEB-200L | |
| Reactor volume | 200L, inner diameter 600mm, outer diameter 650mm, inner length 840mm | |
| Interlayer volume | About 40L | |
| Voltage/Frequency | 220V 50H z/110V 60Hz | |
| S tirring motor power | 750W1/5 | |
| Stirring speed | 0- 280 rpm/min | |
| Temperature range of reactor | -80ºC ~ +250ºC | |
| Temperature measuring accuracy | ±1ºC | |
| Vacuum | 0.098Mpa | |
|
Kettle lid Φ 340mm 6 ports |
Stirring port | Φ 60mm flange port |
| Condens ation refl ux port | 50# ball mill port | |
| Dr opping stark port | 50# ball mill port | |
| Pressure relief port | 34# standard port | |
| Temperature measuring port | Φ 45 mm flange port | |
| Solid feeding port | Φ 80mm flange port , inner diameter Φ 6 0mm matching PTFE cover | |
| Stirring paddle | Φ 20 ×1300 H(mm) blade 240mm | |
| Condenser | Φ 160 mm × 600H(mm), lower Φ 60 mm flange port | |
| Condens ing area | 0.95 | |
| Dean-stark | Upper Φ60 flange port , left 50# ball mill stopper , right 24 # standard port with multi-function valve, lower 50#ball mill plug valve | |
| Dropping flask | 5L barrel shape, upper 29#standard port with air releas ing valve ×2pcs, 34#standard port with glass stopper | |
| Collection flask | 10L, upper 50 #ball mill port , 24#standard port with air releas ing valve ×2pcs, lower glass material releas ing valve | |
| Pressure relief valve | 34# standard plug valve , releasing valve (pagoda joint) with 1 2 mm outer diameter | |
| Material discharg ing port | Φ 100mm flange, Φ 65 mm material discharge hole; oblique discharg ing port (pagoda joint) Φ 40 mm; 3 0 0mm from the ground | |
| Vacuum nozzle | Pagoda joint with 1 2 mm outer diameter | |
| In and out circulating nozzle of condenser coil | Pagoda joint with 1 5 mm outer diameter | |
| Overall dimension (W*D*H) | 1250 ×93 0 × 2800mm | |
| Net weight | 175 KG | |
| Packing dimension |
2200×790×875
mm
1385×880×910
mm
two wooden packages 2.63 m³ |
|
| Packing weight | 271(159+112) KG | |
Pakage&Delivery:
Factory:
Certification: